Titration methods for the determination of hydroxides and carbonates in lithium metal oxide cathode materials

With lithium-ion batteries (LIBs) being one of the most important energy storage technologies today, there is also an increasing need for LIB production to become more sustainable.1 For the anode, aqueous processing has already been realised, eliminating the use of harmful N-methyl-2-pyrrolidone (NMP) during electrode fabrication.2 Unfortunately, the main obstacle to the implementation of aqueous […]

Multi-Chemistry Parameter Sensitivity Analysis of Electrochemical Battery Models

Lithium-ion batteries have become a key element for the decarbonization of the energy and transportation sectors due to their continuously increasing energy and power density as well as decreasing manufacturing and operating costs. Battery models that precisely represent the cell internal states provide the foundation for intelligent control algorithms that accelerate the charging process and, […]

Uncontaminated Preformed SEI on Lithium Metal Electrodes: Impact of Functional Additives

Even though lithium metal has long been regarded as a promising active material for future lithium metal batteries (LMB), the native passivation layers covering pristine lithium metal (pLi) and its possible influence on the evaluation of the solid electrolyte interphase (SEI) has largely been disregarded by the battery research community. The systematic study presented here […]

Silicon@Graphite/Carbon composite anodes: Influence of various pitch derived carbon coatings, Si sizes and concentrations on performance

In the present study the influence of various compositional parameters for a core-shell structured nano-silicon graphite composite (Si@Gr/C) was studied. At first, the stability of the composite particles was evaluated at different silicon contents. It could be observed that an increase in a higher amount of silicon led to reduced composite stability and a detachment […]

Establishment of an extrusion process for the scalable production of sulfide-based SSBs

The focus of this work lies on the establishment of scalable solvent-based processing routes to produce sulfide solid-state cathodes and separators. Sulfide-based solid-state batteries are predicted to have several advantages compared to conventional lithium ion batteries, e.g. in the aspects of energy density, electrochemical stability and safety. These are faced with challenges regarding the formation […]

Comparison of active and passive fillers for the enhancement of the ionic conductivity of polymer-based electrolytes for solid-state batteries

All-solid-state batteries (ASSBs) based on solid polymer electrolytes are among the most promising candidates for next-generation batteries because of their improved safety and energy storage performance. However, the low ionic conductivity of polymer electrolytes at ambient temperature is their main limitation. Hybrid solid electrolytes (HSE) constituted of an organic polymer matrix and an inorganic filler […]

Challenges of Synthesizing Ni-rich ‘Single Crystal’ Layered Oxide Cathodes for Lithium Ion Batteries

Secondary particle cracking has been identified as a major failure mechanism in Ni rich NCMs (Li[NixCoyMnz]O2 with x ≥ 0.8; x+y+z=1) layered oxides as it allows surface-related degradation phenomena such as ongoing electrolyte decomposition on newly formed, highly reactive surface cycle after cycle. As opposed to their polycrystalline (PC) counterparts, ‘Single-crystal’ (SC) NCMs are comprised […]

Challenges of Synthesizing Ni-rich ‘Single Crystal’ Layered Oxide Cathodes for Lithium Ion Batteries

Secondary particle cracking has been identified as a major failure mechanism in Ni rich NCMs (Li[NixCoyMnz]O2 with x ≥ 0.8; x+y+z=1) layered oxides as it allows surface-related degradation phenomena such as ongoing electrolyte decomposition on newly formed, highly reactive surface cycle after cycle. As opposed to their polycrystalline (PC) counterparts, ‘Single-crystal’ (SC) NCMs are comprised […]